The molecular pathway to ZIF-7 microrods revealed by in situ time-resolved small- and wide-angle X-ray scattering, quick-scanning extended X-ray absorption spectroscopy, and DFT calculations

M. Goesten, E. Stavitski, E.A. Pidko, C. Gücüyener, E. Boshuizen, S.N. Ehrlich, E.J.M. Hensen, F. Kapteijn, J. Gascon

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34 Citaten (Scopus)
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Samenvatting

We present an in situ small- and wide-angle X-ray scattering (SAXS/WAXS) and quick-scanning extended X-ray absorption fine-structure (QEXAFS) spectroscopy study on the crystallization of the metal–organic framework ZIF-7. In combination with DFT calculations, the self-assembly and growth of ZIF-7 microrods together with the chemical function of the crystal growth modulator (diethylamine) are revealed at all relevant length scales, from the atomic to the full crystal size.
Originele taal-2Engels
Pagina's (van-tot)7809-7816
Aantal pagina's8
TijdschriftChemistry : A European Journal
Volume19
Nummer van het tijdschrift24
DOI's
StatusGepubliceerd - 2013

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