Stability of zeolite supported (promoted-) Pd catalysts in the reduction of NOx in gas engines using methane

J.A.Z. Pieterse, R.W. Brink, van den, S. Booneveld, F.A. Bruijn, de

Onderzoeksoutput: Hoofdstuk in Boek/Rapport/CongresprocedureConferentiebijdrageAcademicpeer review

6 Citaten (Scopus)

Samenvatting

Zeolite-based palladium catalysts show high activity in the reduction of NOx with methane. The addition of cobalt can further improve the SCR activity up to a level required for 'end-of-pipe' applications in gas engines. However, the hydro-thermal stability of the zeolite supported palladium catalysts is poor. CO-chemisorption, H-2-TPR, DRIFT and activity measurements indicate a temperature-induced mechanism of ion migration and sintering to be the ruling mechanism of deactivation. In addition, the process of steam dealumination under reaction conditions likely eases the sintering. Time on stream behaviour of cobalt-palladium-zeolite equals that of palladium-zeolites. Deactivated catalysts are characterised by a palladium peak in the H-2-TPR at lower temperature as compared to the fresh calcined samples. Cerium (and some other additives) stabilises the active I'd species in mordenite to a significant extent. The mechanism of stabilisation is possibly of both steric and electronic nature.
Originele taal-2Engels
TitelRecent advances in the science and technology of zeolites and related materials : proceedings of the 14th International Zeolite Conference, Cape Town, South Africa, 25-30th April 2004
RedacteurenE. Steen, van der
Plaats van productieAmsterdam
UitgeverijElsevier
Pagina's2522-2526
ISBN van geprinte versie0-444-51805-3
DOI's
StatusGepubliceerd - 2004
Evenementconference; 14th International Zeolite Conference, Cape Town, South Africa, 25-30th April 2004; 2004-04-25; 2004-04-30 -
Duur: 25 apr. 200430 apr. 2004

Publicatie series

NaamStudies in Surface Science and Catalysis
Volume154
ISSN van geprinte versie0167-2991

Congres

Congresconference; 14th International Zeolite Conference, Cape Town, South Africa, 25-30th April 2004; 2004-04-25; 2004-04-30
Periode25/04/0430/04/04
Ander14th International Zeolite Conference, Cape Town, South Africa, 25-30th April 2004

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