Micro reactor application for the Beckmann rearrangement to ε-Caprolactam

K.T. Zuidhof; M.H.J.M. Croon, de; J.C. Schouten

Micro reactor application for the Beckmann rearrangement to ε-Caprolactam

K.T. Zuidhof, M.H.J.M. Croon, de, J.C. Schouten

Chemical Reactor Engineering

Onderzoeksoutput: Hoofdstuk in Boek/Rapport/Congresprocedure › Conferentiebijdrage › Academic › peer review

Samenvatting

Mass and heat transfer can put significant technological limitations to reactor and process design, which leads to far from ideal solutions for bulk processes. A discussion covers the design, construction, and testing of a single channel micro reactor integrated with a micro mixer to demonstrate the viability of a miniaturized reactor system for an industrial bulk process, based on micro reaction technological considerations; model reaction used, i.e., Beckmann rearrangement of cyclohexanone oxime to epsilon-caprolactam with oleum as a catalyst and solvent; the reaction mixture (consisting of caprolactam and oleum) as the key step in the industrial process; window of operation; critical parameters in mass transport models; and the creation of multi micro zones of oxime and oleum rich phases. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).

Originele taal-2	Engels
Titel	Proceedings of the 10th International Conference on Microreaction Technology (IMRET-10), April, 06-10 2008, New Orleans, La
Plaats van productie	New York, NY
Uitgeverij	American Institute of Chemical Engineers (AIChE)
Pagina's	83f-
ISBN van geprinte versie	978-0-8169-1023-6
Status	Gepubliceerd - 2008
Evenement	10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting - New Orleans, LA, Verenigde Staten van Amerika Duur: 1 apr. 2008 → 4 apr. 2008 Congresnummer: 410

Congres

Congres	10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting
Verkorte titel	IMRET 2008
Land/Regio	Verenigde Staten van Amerika
Stad	New Orleans, LA
Periode	1/04/08 → 4/04/08
Ander	AIChE spring national meeting ; (New Orleans, La.) : 2008.04.06-10

Citeer dit

@inproceedings{93d6c1f849bd4fadb9f6b3a620373747,

title = "Micro reactor application for the Beckmann rearrangement to ε-Caprolactam",

abstract = "Mass and heat transfer can put significant technological limitations to reactor and process design, which leads to far from ideal solutions for bulk processes. A discussion covers the design, construction, and testing of a single channel micro reactor integrated with a micro mixer to demonstrate the viability of a miniaturized reactor system for an industrial bulk process, based on micro reaction technological considerations; model reaction used, i.e., Beckmann rearrangement of cyclohexanone oxime to epsilon-caprolactam with oleum as a catalyst and solvent; the reaction mixture (consisting of caprolactam and oleum) as the key step in the industrial process; window of operation; critical parameters in mass transport models; and the creation of multi micro zones of oxime and oleum rich phases. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).",

author = "K.T. Zuidhof and {Croon, de}, M.H.J.M. and J.C. Schouten",

year = "2008",

language = "English",

isbn = "978-0-8169-1023-6",

pages = "83f--",

booktitle = "Proceedings of the 10th International Conference on Microreaction Technology (IMRET-10), April, 06-10 2008, New Orleans, La",

publisher = "American Institute of Chemical Engineers (AIChE)",

address = "United States",

note = "10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting, IMRET 2008 ; Conference date: 01-04-2008 Through 04-04-2008",

}

Zuidhof, KT, Croon, de, MHJM & Schouten, JC 2008, Micro reactor application for the Beckmann rearrangement to ε-Caprolactam. in Proceedings of the 10th International Conference on Microreaction Technology (IMRET-10), April, 06-10 2008, New Orleans, La. American Institute of Chemical Engineers (AIChE), New York, NY, blz. 83f-, 10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting, New Orleans, LA, Verenigde Staten van Amerika, 1/04/08.

Micro reactor application for the Beckmann rearrangement to ε-Caprolactam. / Zuidhof, K.T.; Croon, de, M.H.J.M.; Schouten, J.C.
Proceedings of the 10th International Conference on Microreaction Technology (IMRET-10), April, 06-10 2008, New Orleans, La. New York, NY: American Institute of Chemical Engineers (AIChE), 2008. blz. 83f-.

Onderzoeksoutput: Hoofdstuk in Boek/Rapport/Congresprocedure › Conferentiebijdrage › Academic › peer review

TY - GEN

T1 - Micro reactor application for the Beckmann rearrangement to ε-Caprolactam

AU - Zuidhof, K.T.

AU - Croon, de, M.H.J.M.

AU - Schouten, J.C.

N1 - Conference code: 410

PY - 2008

Y1 - 2008

N2 - Mass and heat transfer can put significant technological limitations to reactor and process design, which leads to far from ideal solutions for bulk processes. A discussion covers the design, construction, and testing of a single channel micro reactor integrated with a micro mixer to demonstrate the viability of a miniaturized reactor system for an industrial bulk process, based on micro reaction technological considerations; model reaction used, i.e., Beckmann rearrangement of cyclohexanone oxime to epsilon-caprolactam with oleum as a catalyst and solvent; the reaction mixture (consisting of caprolactam and oleum) as the key step in the industrial process; window of operation; critical parameters in mass transport models; and the creation of multi micro zones of oxime and oleum rich phases. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).

AB - Mass and heat transfer can put significant technological limitations to reactor and process design, which leads to far from ideal solutions for bulk processes. A discussion covers the design, construction, and testing of a single channel micro reactor integrated with a micro mixer to demonstrate the viability of a miniaturized reactor system for an industrial bulk process, based on micro reaction technological considerations; model reaction used, i.e., Beckmann rearrangement of cyclohexanone oxime to epsilon-caprolactam with oleum as a catalyst and solvent; the reaction mixture (consisting of caprolactam and oleum) as the key step in the industrial process; window of operation; critical parameters in mass transport models; and the creation of multi micro zones of oxime and oleum rich phases. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).

M3 - Conference contribution

SN - 978-0-8169-1023-6

SP - 83f-

BT - Proceedings of the 10th International Conference on Microreaction Technology (IMRET-10), April, 06-10 2008, New Orleans, La

PB - American Institute of Chemical Engineers (AIChE)

CY - New York, NY

T2 - 10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting

Y2 - 1 April 2008 through 4 April 2008

ER -

Micro reactor application for the Beckmann rearrangement to ε-Caprolactam

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Congres

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