USAXS and x-ray microscopy investigation on silica and precursors of zeolites

T.P.M. Beelen; W.H. Dokter; H.F. Garderen, van; R.A. Santen, van; M.T. Browne; G.R. Morrison

USAXS and x-ray microscopy investigation on silica and precursors of zeolites

T.P.M. Beelen, W.H. Dokter, H.F. Garderen, van, R.A. Santen, van, M.T. Browne, G.R. Morrison

Inorganic Materials & Catalysis

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic

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Abstract

Combination of SAXS and USAXS measurements provide an extended q-range (0.006-3.0/nm) to study fractal growth of both aging silica gel as well as precursors of zeolite-A. Mass (silica) and surface (zeolite) fractals are obsd. Scanning transmission X-ray microscopy (STXM) proves to be an extremely useful technique to obtain direct images of wet samples in the 0.1-100 m range, confirming the SAXS/USAXS results on even larger length scales

Original language	English
Title of host publication	Title: Better ceramics through chemistry V : symposium held April 27 - May 1, 1992, San Francisco, California, USA / [Symposium Better Ceramics through Chemistry V].
Editors	M.J.M. Treacy
Place of Publication	Pittsburgh, Pa.
Publisher	Materials Research Society
Pages	263-268
ISBN (Print)	1-558-99166-2
Publication status	Published - 1992
Event	Better Ceramics through Chemistry V, April 27-May 1, 1992, San Francisco, CA, USA - San Francisco, CA, United States Duration: 27 Apr 1992 → 1 May 1992

Publication series

Name	Materials Research Society Symposium Proceedings
Volume	271
ISSN (Print)	0272-9172

Conference

Conference	Better Ceramics through Chemistry V, April 27-May 1, 1992, San Francisco, CA, USA
Country	United States
City	San Francisco, CA
Period	27/04/92 → 1/05/92
Other	Symposium held at the 1992 MRS Spring Meeting

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Beelen, T. P. M., Dokter, W. H., Garderen, van, H. F., Santen, van, R. A., Browne, M. T., & Morrison, G. R. (1992). USAXS and x-ray microscopy investigation on silica and precursors of zeolites. In M. J. M. Treacy (Ed.), Title: Better ceramics through chemistry V : symposium held April 27 - May 1, 1992, San Francisco, California, USA / [Symposium Better Ceramics through Chemistry V]. (pp. 263-268). (Materials Research Society Symposium Proceedings; Vol. 271). Materials Research Society.

Beelen, T.P.M. ; Dokter, W.H. ; Garderen, van, H.F. ; Santen, van, R.A. ; Browne, M.T. ; Morrison, G.R. / USAXS and x-ray microscopy investigation on silica and precursors of zeolites. Title: Better ceramics through chemistry V : symposium held April 27 - May 1, 1992, San Francisco, California, USA / [Symposium Better Ceramics through Chemistry V].. editor / M.J.M. Treacy. Pittsburgh, Pa. : Materials Research Society, 1992. pp. 263-268 (Materials Research Society Symposium Proceedings).

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abstract = "Combination of SAXS and USAXS measurements provide an extended q-range (0.006-3.0/nm) to study fractal growth of both aging silica gel as well as precursors of zeolite-A. Mass (silica) and surface (zeolite) fractals are obsd. Scanning transmission X-ray microscopy (STXM) proves to be an extremely useful technique to obtain direct images of wet samples in the 0.1-100 m range, confirming the SAXS/USAXS results on even larger length scales",

author = "T.P.M. Beelen and W.H. Dokter and {Garderen, van}, H.F. and {Santen, van}, R.A. and M.T. Browne and G.R. Morrison",

year = "1992",

language = "English",

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series = "Materials Research Society Symposium Proceedings",

publisher = "Materials Research Society",

pages = "263--268",

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booktitle = "Title: Better ceramics through chemistry V : symposium held April 27 - May 1, 1992, San Francisco, California, USA / [Symposium Better Ceramics through Chemistry V].",

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note = "Better Ceramics through Chemistry V, April 27-May 1, 1992, San Francisco, CA, USA ; Conference date: 27-04-1992 Through 01-05-1992",

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Beelen, TPM, Dokter, WH, Garderen, van, HF, Santen, van, RA, Browne, MT & Morrison, GR 1992, USAXS and x-ray microscopy investigation on silica and precursors of zeolites. in MJM Treacy (ed.), Title: Better ceramics through chemistry V : symposium held April 27 - May 1, 1992, San Francisco, California, USA / [Symposium Better Ceramics through Chemistry V].. Materials Research Society Symposium Proceedings, vol. 271, Materials Research Society, Pittsburgh, Pa., pp. 263-268, Better Ceramics through Chemistry V, April 27-May 1, 1992, San Francisco, CA, USA , San Francisco, CA, United States, 27/04/92.

USAXS and x-ray microscopy investigation on silica and precursors of zeolites. / Beelen, T.P.M.; Dokter, W.H.; Garderen, van, H.F.; Santen, van, R.A.; Browne, M.T.; Morrison, G.R.

Title: Better ceramics through chemistry V : symposium held April 27 - May 1, 1992, San Francisco, California, USA / [Symposium Better Ceramics through Chemistry V].. ed. / M.J.M. Treacy. Pittsburgh, Pa. : Materials Research Society, 1992. p. 263-268 (Materials Research Society Symposium Proceedings; Vol. 271).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic

TY - GEN

T1 - USAXS and x-ray microscopy investigation on silica and precursors of zeolites

AU - Beelen, T.P.M.

AU - Dokter, W.H.

AU - Garderen, van, H.F.

AU - Santen, van, R.A.

AU - Browne, M.T.

AU - Morrison, G.R.

PY - 1992

Y1 - 1992

N2 - Combination of SAXS and USAXS measurements provide an extended q-range (0.006-3.0/nm) to study fractal growth of both aging silica gel as well as precursors of zeolite-A. Mass (silica) and surface (zeolite) fractals are obsd. Scanning transmission X-ray microscopy (STXM) proves to be an extremely useful technique to obtain direct images of wet samples in the 0.1-100 m range, confirming the SAXS/USAXS results on even larger length scales

AB - Combination of SAXS and USAXS measurements provide an extended q-range (0.006-3.0/nm) to study fractal growth of both aging silica gel as well as precursors of zeolite-A. Mass (silica) and surface (zeolite) fractals are obsd. Scanning transmission X-ray microscopy (STXM) proves to be an extremely useful technique to obtain direct images of wet samples in the 0.1-100 m range, confirming the SAXS/USAXS results on even larger length scales

M3 - Conference contribution

SN - 1-558-99166-2

T3 - Materials Research Society Symposium Proceedings

SP - 263

EP - 268

BT - Title: Better ceramics through chemistry V : symposium held April 27 - May 1, 1992, San Francisco, California, USA / [Symposium Better Ceramics through Chemistry V].

A2 - Treacy, M.J.M.

PB - Materials Research Society

CY - Pittsburgh, Pa.

T2 - Better Ceramics through Chemistry V, April 27-May 1, 1992, San Francisco, CA, USA

Y2 - 27 April 1992 through 1 May 1992

ER -

Beelen TPM, Dokter WH, Garderen, van HF, Santen, van RA, Browne MT, Morrison GR. USAXS and x-ray microscopy investigation on silica and precursors of zeolites. In Treacy MJM, editor, Title: Better ceramics through chemistry V : symposium held April 27 - May 1, 1992, San Francisco, California, USA / [Symposium Better Ceramics through Chemistry V].. Pittsburgh, Pa.: Materials Research Society. 1992. p. 263-268. (Materials Research Society Symposium Proceedings).