The effects of drying, aging and curing on an organic-inorganic coating

J. Malzbender, G. With, de

Research output: Contribution to journalArticleAcademicpeer-review

14 Citations (Scopus)
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Abstract

The effects of drying, aging and curing on an organic - inorganic coating deposited on float glass substrates were analyzed. Methyltrimethoxysilane was used to immobilize parts of the network connections and silica particles were used as seeds for the nucleation of the gel structure. The coating was produced under acidic conditions to enhance the hydrolysis reaction. The coatings were deposited using a spin-coating technique. The dependence of the elastic modulus, hardness, fracture toughness and residual stress obtained by indentation on the preparation conditions is reported. In addition results obtained by X-ray diffraction (XRD), Atomic Force Microscopy (AFM), X-ray Photon Spectroscopy (XPS) and Infrared-Spectroscopy are analyzed.
Original languageEnglish
Pages (from-to)4809-4814
Number of pages15
JournalJournal of Materials Science
Volume35
Issue number19
DOIs
Publication statusPublished - 2000

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Inorganic coatings
Organic coatings
Curing
Drying
Aging of materials
Spectroscopy
Coatings
Coating techniques
Spin coating
Silicon Dioxide
Seed
Fracture toughness
Residual stresses
Atomic force microscopy
Nucleation
Photons
Elastic moduli
Hardness
Silica
X rays

Cite this

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title = "The effects of drying, aging and curing on an organic-inorganic coating",
abstract = "The effects of drying, aging and curing on an organic - inorganic coating deposited on float glass substrates were analyzed. Methyltrimethoxysilane was used to immobilize parts of the network connections and silica particles were used as seeds for the nucleation of the gel structure. The coating was produced under acidic conditions to enhance the hydrolysis reaction. The coatings were deposited using a spin-coating technique. The dependence of the elastic modulus, hardness, fracture toughness and residual stress obtained by indentation on the preparation conditions is reported. In addition results obtained by X-ray diffraction (XRD), Atomic Force Microscopy (AFM), X-ray Photon Spectroscopy (XPS) and Infrared-Spectroscopy are analyzed.",
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pages = "4809--4814",
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The effects of drying, aging and curing on an organic-inorganic coating. / Malzbender, J.; With, de, G.

In: Journal of Materials Science, Vol. 35, No. 19, 2000, p. 4809-4814.

Research output: Contribution to journalArticleAcademicpeer-review

TY - JOUR

T1 - The effects of drying, aging and curing on an organic-inorganic coating

AU - Malzbender, J.

AU - With, de, G.

PY - 2000

Y1 - 2000

N2 - The effects of drying, aging and curing on an organic - inorganic coating deposited on float glass substrates were analyzed. Methyltrimethoxysilane was used to immobilize parts of the network connections and silica particles were used as seeds for the nucleation of the gel structure. The coating was produced under acidic conditions to enhance the hydrolysis reaction. The coatings were deposited using a spin-coating technique. The dependence of the elastic modulus, hardness, fracture toughness and residual stress obtained by indentation on the preparation conditions is reported. In addition results obtained by X-ray diffraction (XRD), Atomic Force Microscopy (AFM), X-ray Photon Spectroscopy (XPS) and Infrared-Spectroscopy are analyzed.

AB - The effects of drying, aging and curing on an organic - inorganic coating deposited on float glass substrates were analyzed. Methyltrimethoxysilane was used to immobilize parts of the network connections and silica particles were used as seeds for the nucleation of the gel structure. The coating was produced under acidic conditions to enhance the hydrolysis reaction. The coatings were deposited using a spin-coating technique. The dependence of the elastic modulus, hardness, fracture toughness and residual stress obtained by indentation on the preparation conditions is reported. In addition results obtained by X-ray diffraction (XRD), Atomic Force Microscopy (AFM), X-ray Photon Spectroscopy (XPS) and Infrared-Spectroscopy are analyzed.

U2 - 10.1023/A:1004824812867

DO - 10.1023/A:1004824812867

M3 - Article

VL - 35

SP - 4809

EP - 4814

JO - Journal of Materials Science

JF - Journal of Materials Science

SN - 0022-2461

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ER -