Synthesis of O-methyl thioformate

D.H. Holsboer; H. Kloosterziel

doi:10.1002/recl.19720911114

Synthesis of O-methyl thioformate

D.H. Holsboer, H. Kloosterziel

Chemical Engineering and Chemistry

Research output: Contribution to journal › Article › Academic › peer-review

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Abstract

HC(S)OMe (I) was prepd. from MeOCHCl2 (II) and EtOC(S)SK (III) via EtOC(S)SCH(OMe)SC(S)OEt. Thus, II was added to III in EtOH and the crude product heated at 200-20 Deg to give EtOC(S)SEt and 56% I. [on SciFinder (R)]

Original language	English
Pages (from-to)	1371-1372
Journal	Recueil des Travaux Chimiques des Pays-Bas
Volume	91
Issue number	11
DOIs	https://doi.org/10.1002/recl.19720911114
Publication status	Published - 1972

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10.1002/recl.19720911114

Cite this

@article{f0224d46c638449fb19b3f592833469c,

title = "Synthesis of O-methyl thioformate",

abstract = "HC(S)OMe (I) was prepd. from MeOCHCl2 (II) and EtOC(S)SK (III) via EtOC(S)SCH(OMe)SC(S)OEt. Thus, II was added to III in EtOH and the crude product heated at 200-20 Deg to give EtOC(S)SEt and 56% I. [on SciFinder (R)]",

author = "D.H. Holsboer and H. Kloosterziel",

year = "1972",

doi = "10.1002/recl.19720911114",

language = "English",

volume = "91",

pages = "1371--1372",

journal = "Recueil des Travaux Chimiques des Pays-Bas",

issn = "0165-0513",

publisher = "Royal Netherlands Chemical Society",

number = "11",

}

TY - JOUR

T1 - Synthesis of O-methyl thioformate

AU - Holsboer, D.H.

AU - Kloosterziel, H.

PY - 1972

Y1 - 1972

N2 - HC(S)OMe (I) was prepd. from MeOCHCl2 (II) and EtOC(S)SK (III) via EtOC(S)SCH(OMe)SC(S)OEt. Thus, II was added to III in EtOH and the crude product heated at 200-20 Deg to give EtOC(S)SEt and 56% I. [on SciFinder (R)]

AB - HC(S)OMe (I) was prepd. from MeOCHCl2 (II) and EtOC(S)SK (III) via EtOC(S)SCH(OMe)SC(S)OEt. Thus, II was added to III in EtOH and the crude product heated at 200-20 Deg to give EtOC(S)SEt and 56% I. [on SciFinder (R)]

U2 - 10.1002/recl.19720911114

DO - 10.1002/recl.19720911114

M3 - Article

VL - 91

SP - 1371

EP - 1372

JO - Recueil des Travaux Chimiques des Pays-Bas

JF - Recueil des Travaux Chimiques des Pays-Bas

SN - 0165-0513

IS - 11

ER -