Synthesis of O-methyl thioformate

D.H. Holsboer, H. Kloosterziel

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Abstract

HC(S)OMe (I) was prepd. from MeOCHCl2 (II) and EtOC(S)SK (III) via EtOC(S)SCH(OMe)SC(S)OEt. Thus, II was added to III in EtOH and the crude product heated at 200-20 Deg to give EtOC(S)SEt and 56% I. [on SciFinder (R)]
Original languageEnglish
Pages (from-to)1371-1372
JournalRecueil des Travaux Chimiques des Pays-Bas
Volume91
Issue number11
DOIs
Publication statusPublished - 1972

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