Structure assignment of isomeric chain demethylated retinals by 1H NMR spectroscopy

A.D. Broek; J.M.C. Courtin; J.R. Mellema; J. Lugtenburg; K. Nicolaij; K. Dijkstra; R. Kaptein

doi:10.1002/mrc.1270190213

Structure assignment of isomeric chain demethylated retinals by 1H NMR spectroscopy

A.D. Broek, J.M.C. Courtin, J.R. Mellema, J. Lugtenburg, K. Nicolaij, K. Dijkstra, R. Kaptein

Biomedical NMR

Research output: Contribution to journal › Article › Academic › peer-review

6 Citations (Scopus)

Abstract

Geometric isomers of all-trans-9-demethyl-, -13-demethyl- and -9,13-bisdemethylretinal were prepared. The 360 MHz 1H NMR spectra of 13 geometric isomers of these three demethylated retinal systems have been measured. The chemical shift and coupling constant values in each case allowed an unambiguous assignment of the structure of each compound.

Original language	English
Pages (from-to)	105-107
Journal	Organic Magnetic Resonance
Volume	19
Issue number	2
DOIs	https://doi.org/10.1002/mrc.1270190213
Publication status	Published - 1982

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title = "Structure assignment of isomeric chain demethylated retinals by 1H NMR spectroscopy",

abstract = "Geometric isomers of all-trans-9-demethyl-, -13-demethyl- and -9,13-bisdemethylretinal were prepared. The 360 MHz 1H NMR spectra of 13 geometric isomers of these three demethylated retinal systems have been measured. The chemical shift and coupling constant values in each case allowed an unambiguous assignment of the structure of each compound.",

author = "A.D. Broek and J.M.C. Courtin and J.R. Mellema and J. Lugtenburg and K. Nicolaij and K. Dijkstra and R. Kaptein",

year = "1982",

doi = "10.1002/mrc.1270190213",

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journal = "Organic Magnetic Resonance",

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T1 - Structure assignment of isomeric chain demethylated retinals by 1H NMR spectroscopy

AU - Broek, A.D.

AU - Courtin, J.M.C.

AU - Mellema, J.R.

AU - Lugtenburg, J.

AU - Nicolaij, K.

AU - Dijkstra, K.

AU - Kaptein, R.

PY - 1982

Y1 - 1982

N2 - Geometric isomers of all-trans-9-demethyl-, -13-demethyl- and -9,13-bisdemethylretinal were prepared. The 360 MHz 1H NMR spectra of 13 geometric isomers of these three demethylated retinal systems have been measured. The chemical shift and coupling constant values in each case allowed an unambiguous assignment of the structure of each compound.

AB - Geometric isomers of all-trans-9-demethyl-, -13-demethyl- and -9,13-bisdemethylretinal were prepared. The 360 MHz 1H NMR spectra of 13 geometric isomers of these three demethylated retinal systems have been measured. The chemical shift and coupling constant values in each case allowed an unambiguous assignment of the structure of each compound.

U2 - 10.1002/mrc.1270190213

DO - 10.1002/mrc.1270190213

M3 - Article

VL - 19

SP - 105

EP - 107

JO - Organic Magnetic Resonance

JF - Organic Magnetic Resonance

SN - 0030-4921

IS - 2

ER -