Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study

W.H. Dokter; T.P.M. Beelen; H.F. Garderen, van; R.A. Santen, van; W. Bras; G.E. Derbyshire; G.R. Mant

doi:10.1107/S0021889894004693

Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study

W.H. Dokter
, T.P.M. Beelen
, H.F. Garderen, van
, R.A. Santen, van
, W. Bras
, G.E. Derbyshire
, G.R. Mant

Research output: Contribution to journal › Article › Academic › peer-review

43 Citations (Scopus)

137 Downloads (Pure)

Abstract

The gel transformations and subsequent crystn. that occur in the precursor reaction mixt. of silicalite were studied using simultaneous small- and wide-angle x-ray scattering (SAXS-WAXS). The SAXS-WAXS measurements, together using a high flux of synchrotron radiation and a newly developed high-pressure reaction cell, provide the possibility of in situ hydrothermal and time-resolved monitoring of amorphous gel transformations and crystn. [on SciFinder (R)]

Original language	English
Pages (from-to)	901-906
Number of pages	6
Journal	Journal of Applied Crystallography
Volume	27
Issue number	6
DOIs	https://doi.org/10.1107/S0021889894004693
Publication status	Published - 1994

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Dokter, W. H., Beelen, T. P. M., Garderen, van, H. F., Santen, van, R. A., Bras, W., Derbyshire, G. E., & Mant, G. R. (1994). Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study. Journal of Applied Crystallography, 27(6), 901-906. https://doi.org/10.1107/S0021889894004693

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title = "Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study",

abstract = "The gel transformations and subsequent crystn. that occur in the precursor reaction mixt. of silicalite were studied using simultaneous small- and wide-angle x-ray scattering (SAXS-WAXS). The SAXS-WAXS measurements, together using a high flux of synchrotron radiation and a newly developed high-pressure reaction cell, provide the possibility of in situ hydrothermal and time-resolved monitoring of amorphous gel transformations and crystn. [on SciFinder (R)]",

author = "W.H. Dokter and T.P.M. Beelen and \{Garderen, van\}, H.F. and \{Santen, van\}, R.A. and W. Bras and G.E. Derbyshire and G.R. Mant",

year = "1994",

doi = "10.1107/S0021889894004693",

language = "English",

volume = "27",

pages = "901--906",

journal = "Journal of Applied Crystallography",

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publisher = "International Union of Crystallography",

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Dokter, WH, Beelen, TPM, Garderen, van, HF, Santen, van, RA, Bras, W, Derbyshire, GE & Mant, GR 1994, 'Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study', Journal of Applied Crystallography, vol. 27, no. 6, pp. 901-906. https://doi.org/10.1107/S0021889894004693

Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study. / Dokter, W.H.; Beelen, T.P.M.; Garderen, van, H.F. et al.
In: Journal of Applied Crystallography, Vol. 27, No. 6, 1994, p. 901-906.

Research output: Contribution to journal › Article › Academic › peer-review

TY - JOUR

T1 - Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study

AU - Dokter, W.H.

AU - Beelen, T.P.M.

AU - Garderen, van, H.F.

AU - Santen, van, R.A.

AU - Bras, W.

AU - Derbyshire, G.E.

AU - Mant, G.R.

PY - 1994

Y1 - 1994

N2 - The gel transformations and subsequent crystn. that occur in the precursor reaction mixt. of silicalite were studied using simultaneous small- and wide-angle x-ray scattering (SAXS-WAXS). The SAXS-WAXS measurements, together using a high flux of synchrotron radiation and a newly developed high-pressure reaction cell, provide the possibility of in situ hydrothermal and time-resolved monitoring of amorphous gel transformations and crystn. [on SciFinder (R)]

AB - The gel transformations and subsequent crystn. that occur in the precursor reaction mixt. of silicalite were studied using simultaneous small- and wide-angle x-ray scattering (SAXS-WAXS). The SAXS-WAXS measurements, together using a high flux of synchrotron radiation and a newly developed high-pressure reaction cell, provide the possibility of in situ hydrothermal and time-resolved monitoring of amorphous gel transformations and crystn. [on SciFinder (R)]

U2 - 10.1107/S0021889894004693

DO - 10.1107/S0021889894004693

M3 - Article

SN - 0021-8898

VL - 27

SP - 901

EP - 906

JO - Journal of Applied Crystallography

JF - Journal of Applied Crystallography

IS - 6

ER -

Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study

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