Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle x-ray scattering study

W.H. Dokter, T.P.M. Beelen, H.F. Garderen, van, R.A. Santen, van, W. Bras, G.E. Derbyshire, G.R. Mant

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Abstract

The gel transformations and subsequent crystn. that occur in the precursor reaction mixt. of silicalite were studied using simultaneous small- and wide-angle x-ray scattering (SAXS-WAXS). The SAXS-WAXS measurements, together using a high flux of synchrotron radiation and a newly developed high-pressure reaction cell, provide the possibility of in situ hydrothermal and time-resolved monitoring of amorphous gel transformations and crystn. [on SciFinder (R)]
Original languageEnglish
Pages (from-to)901-906
JournalJournal of Applied Crystallography
Volume27
Issue number6
DOIs
Publication statusPublished - 1994

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