Rheological characterization of waxy crude oils: Sample preparation

Flávio H. Marchesini, Alexandra A. Alicke, Paulo R. De Souza Mendes, Cláudio M. Ziglio

Research output: Contribution to journalArticleAcademicpeer-review

67 Citations (Scopus)

Abstract

In this paper, we describe an experimental protocol designed to ensure well-defined thermal and shear histories of a waxy crude oil sample to be submitted to rheological measurements. We discuss the criteria for choosing an appropriate pretreatment, the geometry, and the temperature range, among other parameters. This protocol includes the so-called thermal cycle test, which is shown to play a key role in determining the appropriate test conditions. Possible sources of measurement error are discussed in detail.

Original languageEnglish
Pages (from-to)2566-2577
Number of pages12
JournalEnergy & Fuels
Volume26
Issue number5
DOIs
Publication statusPublished - 17 May 2012
Externally publishedYes

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