Optimization of capillary SFC-MS for the determination of additives in polymers

R.G.J. Leuken, van, M.A.A. Mertens, J.G.M. Janssen, P.J.F. Sandra, G. Kwakkenbos, R.S. Deelder

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Abstract

A standard direct introduction capillary interface is used for the SFC-MS analysis of polymer additives. The system is optimized with respect to the position of the restrictor, probe tip temperature, and ion source temperature. El-like charge-exchange spectra are obtained. Cl using ammonia as the reagent gas is used for the quantitative analysis of a real world sample. The experimental capillary SFC-MS spectra obtained show a good similarity with those recorded using the direct insertion probe. The influence of the experimental conditions on the mass spectra obtained is evaluated statistically.
Original languageEnglish
Pages (from-to)573-576
Number of pages4
JournalJournal of High Resolution Chromatography
Volume17
Issue number8
DOIs
Publication statusPublished - 1994

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