Open hole tubular columns in pesticide analysis

J.J. Franken, H. Vader

Research output: Contribution to journalArticleAcademicpeer-review

12 Citations (Scopus)

Abstract

The combination of the high resolving power of capillary columns and the extreme sensitivity of the electron capture detector gives us a powerful tool for the analysis of chlorinated pesticides. The connection of capillary columns to gas chromatographic equipment not speically designed for these, requires special adaptations. A generally suitable connection for capillary columns to injection ports and to the Hewlett Packard electron capture detector is described. The preparation of capillary columns suitable for pesticide analyses is discussed. Results obtained with synthetic mixtures and with biological samples are given. The equipment as described, proved to be suitable and reliable for the analysis of chlorinated pesticides.
Original languageEnglish
Pages (from-to)22-27
Number of pages6
JournalChromatographia
Volume6
Issue number1
DOIs
Publication statusPublished - 1973

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Pesticides
Detectors
Electrons
Optical resolving power
Equipment and Supplies
Gases
Injections

Cite this

Franken, J.J. ; Vader, H. / Open hole tubular columns in pesticide analysis. In: Chromatographia. 1973 ; Vol. 6, No. 1. pp. 22-27.
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Open hole tubular columns in pesticide analysis. / Franken, J.J.; Vader, H.

In: Chromatographia, Vol. 6, No. 1, 1973, p. 22-27.

Research output: Contribution to journalArticleAcademicpeer-review

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AU - Franken, J.J.

AU - Vader, H.

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N2 - The combination of the high resolving power of capillary columns and the extreme sensitivity of the electron capture detector gives us a powerful tool for the analysis of chlorinated pesticides. The connection of capillary columns to gas chromatographic equipment not speically designed for these, requires special adaptations. A generally suitable connection for capillary columns to injection ports and to the Hewlett Packard electron capture detector is described. The preparation of capillary columns suitable for pesticide analyses is discussed. Results obtained with synthetic mixtures and with biological samples are given. The equipment as described, proved to be suitable and reliable for the analysis of chlorinated pesticides.

AB - The combination of the high resolving power of capillary columns and the extreme sensitivity of the electron capture detector gives us a powerful tool for the analysis of chlorinated pesticides. The connection of capillary columns to gas chromatographic equipment not speically designed for these, requires special adaptations. A generally suitable connection for capillary columns to injection ports and to the Hewlett Packard electron capture detector is described. The preparation of capillary columns suitable for pesticide analyses is discussed. Results obtained with synthetic mixtures and with biological samples are given. The equipment as described, proved to be suitable and reliable for the analysis of chlorinated pesticides.

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