Morphological, structural and conformational changes in polymer systems probed by in-situ techniques

J.G.P. Goossens; S. Rastogi; P.J. Lemstra; H.E.H. Meijer

Morphological, structural and conformational changes in polymer systems probed by in-situ techniques

J.G.P. Goossens, S. Rastogi, P.J. Lemstra, H.E.H. Meijer

Processing and Performance

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

Abstract

The combination of simultaneous SAXS, WAXS, and Raman spectroscopy renders the possibility to follow in-situ morphological, structural and reaction kinetics with a perfect time correlation. This combination has been used to get more insight in the L-S transition and the occurrence of microand macro-phase separation during in-situ polymerisation of styrene starting from a homogeneous solution with polyethylene. The results show that Raman spectroscopy can also be used as an indirect measurement for the change in optical properties of the system, which can be related to the volume of measurement. Particularly interesting is that this kind of turbidity measurements are very sensitive for the onset of crystallisation and the occurrence of micro– and macro phase separation.

Original language	English
Title of host publication	Polymer Processing Society : annual meeting, 15th, 's-Hertogenbosch, The Netherlands, May 31 - June 4, 1999 : proceedings
Editors	P.D. Anderson, P.G.M. Kruit
Publisher	Polymer Processing Society
Publication status	Published - 1999
Event	15th Annual Meeting of the Polymer Processing Society (PPS-15) - 's-Hertogenbosch, Netherlands Duration: 31 May 1999 → 4 Jun 1999 Conference number: 15

Conference

Conference	15th Annual Meeting of the Polymer Processing Society (PPS-15)
Abbreviated title	PPS
Country/Territory	Netherlands
City	's-Hertogenbosch
Period	31/05/99 → 4/06/99

Cite this

Goossens, J. G. P., Rastogi, S., Lemstra, P. J., & Meijer, H. E. H. (1999). Morphological, structural and conformational changes in polymer systems probed by in-situ techniques. In P. D. Anderson, & P. G. M. Kruit (Eds.), Polymer Processing Society : annual meeting, 15th, 's-Hertogenbosch, The Netherlands, May 31 - June 4, 1999 : proceedings Polymer Processing Society.

@inproceedings{c2dcfe55a8bb4cd684de7a4c4dca650b,

title = "Morphological, structural and conformational changes in polymer systems probed by in-situ techniques",

abstract = "The combination of simultaneous SAXS, WAXS, and Raman spectroscopy renders the possibility to follow in-situ morphological, structural and reaction kinetics with a perfect time correlation. This combination has been used to get more insight in the L-S transition and the occurrence of microand macro-phase separation during in-situ polymerisation of styrene starting from a homogeneous solution with polyethylene. The results show that Raman spectroscopy can also be used as an indirect measurement for the change in optical properties of the system, which can be related to the volume of measurement. Particularly interesting is that this kind of turbidity measurements are very sensitive for the onset of crystallisation and the occurrence of micro– and macro phase separation.",

author = "J.G.P. Goossens and S. Rastogi and P.J. Lemstra and H.E.H. Meijer",

year = "1999",

language = "English",

editor = "P.D. Anderson and P.G.M. Kruit",

booktitle = "Polymer Processing Society : annual meeting, 15th, 's-Hertogenbosch, The Netherlands, May 31 - June 4, 1999 : proceedings",

publisher = "Polymer Processing Society",

note = "15th Annual Meeting of the Polymer Processing Society (PPS-15), PPS ; Conference date: 31-05-1999 Through 04-06-1999",

}

Goossens, JGP, Rastogi, S, Lemstra, PJ & Meijer, HEH 1999, Morphological, structural and conformational changes in polymer systems probed by in-situ techniques. in PD Anderson & PGM Kruit (eds), Polymer Processing Society : annual meeting, 15th, 's-Hertogenbosch, The Netherlands, May 31 - June 4, 1999 : proceedings. Polymer Processing Society, 15th Annual Meeting of the Polymer Processing Society (PPS-15), 's-Hertogenbosch, Netherlands, 31/05/99.

Morphological, structural and conformational changes in polymer systems probed by in-situ techniques. / Goossens, J.G.P.; Rastogi, S.; Lemstra, P.J. et al.

Polymer Processing Society : annual meeting, 15th, 's-Hertogenbosch, The Netherlands, May 31 - June 4, 1999 : proceedings. ed. / P.D. Anderson; P.G.M. Kruit. Polymer Processing Society, 1999.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

TY - GEN

T1 - Morphological, structural and conformational changes in polymer systems probed by in-situ techniques

AU - Goossens, J.G.P.

AU - Rastogi, S.

AU - Lemstra, P.J.

AU - Meijer, H.E.H.

N1 - Conference code: 15

PY - 1999

Y1 - 1999

N2 - The combination of simultaneous SAXS, WAXS, and Raman spectroscopy renders the possibility to follow in-situ morphological, structural and reaction kinetics with a perfect time correlation. This combination has been used to get more insight in the L-S transition and the occurrence of microand macro-phase separation during in-situ polymerisation of styrene starting from a homogeneous solution with polyethylene. The results show that Raman spectroscopy can also be used as an indirect measurement for the change in optical properties of the system, which can be related to the volume of measurement. Particularly interesting is that this kind of turbidity measurements are very sensitive for the onset of crystallisation and the occurrence of micro– and macro phase separation.

AB - The combination of simultaneous SAXS, WAXS, and Raman spectroscopy renders the possibility to follow in-situ morphological, structural and reaction kinetics with a perfect time correlation. This combination has been used to get more insight in the L-S transition and the occurrence of microand macro-phase separation during in-situ polymerisation of styrene starting from a homogeneous solution with polyethylene. The results show that Raman spectroscopy can also be used as an indirect measurement for the change in optical properties of the system, which can be related to the volume of measurement. Particularly interesting is that this kind of turbidity measurements are very sensitive for the onset of crystallisation and the occurrence of micro– and macro phase separation.

M3 - Conference contribution

BT - Polymer Processing Society : annual meeting, 15th, 's-Hertogenbosch, The Netherlands, May 31 - June 4, 1999 : proceedings

A2 - Anderson, P.D.

A2 - Kruit, P.G.M.

PB - Polymer Processing Society

T2 - 15th Annual Meeting of the Polymer Processing Society (PPS-15)

Y2 - 31 May 1999 through 4 June 1999

ER -

Morphological, structural and conformational changes in polymer systems probed by in-situ techniques

Abstract

Conference

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