TY - JOUR
T1 - Micromechanical and microstructural properties of tungsten fibers in the as-produced and annealed state
T2 - Assessment of the potassium doping effect
AU - Terentyev, D.
AU - Tanure, L.
AU - Bakaeva, A.
AU - Dubinko, A.
AU - Nikolić, V.
AU - Riesch, J.
AU - Verbeken, K.
AU - Lebediev, S.
AU - Zhurkin, E.E.
PY - 2019/6/1
Y1 - 2019/6/1
N2 -
Due to its high strength and low temperature ductility, tungsten fibers (W
f
) have been widely used as reinforcement elements in metallic, ceramic and glass matrix composites to improve the strength, toughness and creep resistance. Materials designed for future fusion reactors also utilize the option of W
f
reinforcement, i.a. with a copper (W
f
/Cu) or tungsten (W
f
/W) matrix. W
f
/W composites are being intensively studied as risk-mitigation materials to replace bulk tungsten which is susceptible to embrittlement induced by neutrons resulting from fusion reaction. Operation of W
f
/W in high temperatures (up to 1300 °C and even higher) fusion environment implies a risk of recrystallization and grain growth, which dimishes the attractive properties of tungsten fibers. In this work, we assess this modification of micro-mechanical and microstructural properties of tungsten fibers by means of nanoindentation, scanning electron microscopy, electron back-scattering diffraction analysis and corelate it with the ultimate tensile strength and fracture modes observed in the tensile tests. Both pure W and pottasium doped wires in the as-fabricated and annealed states are investigated and the results are compared with bulk tungsten, also exposed to several annealing temperatures. The results highlight the postive impact of potassium doping which shifts the threshold temperature for the grain growth by about 600 °C compared to pure tungsten wire. The results of the nanoindentation revealed systematic linear correlation with the ultimate tensile strength, which therefore offers a complimenatary way of micro-mechanical testing linking it with macro-scale properties of the wires.
AB -
Due to its high strength and low temperature ductility, tungsten fibers (W
f
) have been widely used as reinforcement elements in metallic, ceramic and glass matrix composites to improve the strength, toughness and creep resistance. Materials designed for future fusion reactors also utilize the option of W
f
reinforcement, i.a. with a copper (W
f
/Cu) or tungsten (W
f
/W) matrix. W
f
/W composites are being intensively studied as risk-mitigation materials to replace bulk tungsten which is susceptible to embrittlement induced by neutrons resulting from fusion reaction. Operation of W
f
/W in high temperatures (up to 1300 °C and even higher) fusion environment implies a risk of recrystallization and grain growth, which dimishes the attractive properties of tungsten fibers. In this work, we assess this modification of micro-mechanical and microstructural properties of tungsten fibers by means of nanoindentation, scanning electron microscopy, electron back-scattering diffraction analysis and corelate it with the ultimate tensile strength and fracture modes observed in the tensile tests. Both pure W and pottasium doped wires in the as-fabricated and annealed states are investigated and the results are compared with bulk tungsten, also exposed to several annealing temperatures. The results highlight the postive impact of potassium doping which shifts the threshold temperature for the grain growth by about 600 °C compared to pure tungsten wire. The results of the nanoindentation revealed systematic linear correlation with the ultimate tensile strength, which therefore offers a complimenatary way of micro-mechanical testing linking it with macro-scale properties of the wires.
KW - Annealing
KW - Composites
KW - Fiber
KW - Plasticity
KW - Potassium doped
KW - Recrystallization
KW - Tungsten
UR - http://www.scopus.com/inward/record.url?scp=85062831814&partnerID=8YFLogxK
U2 - 10.1016/j.ijrmhm.2019.03.012
DO - 10.1016/j.ijrmhm.2019.03.012
M3 - Article
AN - SCOPUS:85062831814
SN - 0263-4368
VL - 81
SP - 253
EP - 271
JO - International Journal of Refractory Metals and Hard Materials
JF - International Journal of Refractory Metals and Hard Materials
ER -