Micro reactor application for the Beckmann rearrangement to epsilon-caprolactam

K. T. Zuidhof; D. V. Raulji; M. H.J.M. De Croon; J. C. Schouten

Micro reactor application for the Beckmann rearrangement to epsilon-caprolactam

K. T. Zuidhof, D. V. Raulji, M. H.J.M. De Croon, J. C. Schouten

Chemical Reactor Engineering

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

Abstract

Mass and heat transfer can put significant technological limitations to reactor and process design, which leads to far from ideal solutions for bulk processes. A discussion covers the design, construction, and testing of a single channel micro reactor integrated with a micro mixer to demonstrate the viability of a miniaturized reactor system for an industrial bulk process, based on micro reaction technological considerations; model reaction used, i.e., Beckmann rearrangement of cyclohexanone oxime to epsilon-caprolactam with oleum as a catalyst and solvent; the reaction mixture (consisting of caprolactam and oleum) as the key step in the industrial process; window of operation; critical parameters in mass transport models; and the creation of multi micro zones of oxime and oleum rich phases. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).

Original language	English
Title of host publication	10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting
Publisher	American Institute of Chemical Engineers (AIChE)
Pages	75-76
Number of pages	2
ISBN (Print)	9781605602110
Publication status	Published - 23 Dec 2008
Event	10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting - New Orleans, LA, United States Duration: 1 Apr 2008 → 4 Apr 2008 Conference number: 410

Conference

Conference	10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting
Abbreviated title	IMRET 2008
Country/Territory	United States
City	New Orleans, LA
Period	1/04/08 → 4/04/08
Other	Topical conference at 2008 AIChE Spring Meeting & 4th Global Congress on Process Safety

Cite this

@inproceedings{551e74cab6ac4275b9eae0c79597cc47,

title = "Micro reactor application for the Beckmann rearrangement to epsilon-caprolactam",

abstract = "Mass and heat transfer can put significant technological limitations to reactor and process design, which leads to far from ideal solutions for bulk processes. A discussion covers the design, construction, and testing of a single channel micro reactor integrated with a micro mixer to demonstrate the viability of a miniaturized reactor system for an industrial bulk process, based on micro reaction technological considerations; model reaction used, i.e., Beckmann rearrangement of cyclohexanone oxime to epsilon-caprolactam with oleum as a catalyst and solvent; the reaction mixture (consisting of caprolactam and oleum) as the key step in the industrial process; window of operation; critical parameters in mass transport models; and the creation of multi micro zones of oxime and oleum rich phases. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).",

author = "Zuidhof, {K. T.} and Raulji, {D. V.} and {De Croon}, {M. H.J.M.} and Schouten, {J. C.}",

year = "2008",

month = dec,

day = "23",

language = "English",

isbn = "9781605602110",

pages = "75--76",

booktitle = "10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting",

publisher = "American Institute of Chemical Engineers (AIChE)",

address = "United States",

note = "10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting, IMRET 2008 ; Conference date: 01-04-2008 Through 04-04-2008",

}

Zuidhof, KT, Raulji, DV, De Croon, MHJM & Schouten, JC 2008, Micro reactor application for the Beckmann rearrangement to epsilon-caprolactam. in 10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting. American Institute of Chemical Engineers (AIChE), pp. 75-76, 10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting, New Orleans, LA, United States, 1/04/08.

Micro reactor application for the Beckmann rearrangement to epsilon-caprolactam. / Zuidhof, K. T.; Raulji, D. V.; De Croon, M. H.J.M. et al.
10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting. American Institute of Chemical Engineers (AIChE), 2008. p. 75-76.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

TY - GEN

T1 - Micro reactor application for the Beckmann rearrangement to epsilon-caprolactam

AU - Zuidhof, K. T.

AU - Raulji, D. V.

AU - De Croon, M. H.J.M.

AU - Schouten, J. C.

N1 - Conference code: 410

PY - 2008/12/23

Y1 - 2008/12/23

N2 - Mass and heat transfer can put significant technological limitations to reactor and process design, which leads to far from ideal solutions for bulk processes. A discussion covers the design, construction, and testing of a single channel micro reactor integrated with a micro mixer to demonstrate the viability of a miniaturized reactor system for an industrial bulk process, based on micro reaction technological considerations; model reaction used, i.e., Beckmann rearrangement of cyclohexanone oxime to epsilon-caprolactam with oleum as a catalyst and solvent; the reaction mixture (consisting of caprolactam and oleum) as the key step in the industrial process; window of operation; critical parameters in mass transport models; and the creation of multi micro zones of oxime and oleum rich phases. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).

AB - Mass and heat transfer can put significant technological limitations to reactor and process design, which leads to far from ideal solutions for bulk processes. A discussion covers the design, construction, and testing of a single channel micro reactor integrated with a micro mixer to demonstrate the viability of a miniaturized reactor system for an industrial bulk process, based on micro reaction technological considerations; model reaction used, i.e., Beckmann rearrangement of cyclohexanone oxime to epsilon-caprolactam with oleum as a catalyst and solvent; the reaction mixture (consisting of caprolactam and oleum) as the key step in the industrial process; window of operation; critical parameters in mass transport models; and the creation of multi micro zones of oxime and oleum rich phases. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).

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M3 - Conference contribution

SN - 9781605602110

SP - 75

EP - 76

BT - 10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting

PB - American Institute of Chemical Engineers (AIChE)

T2 - 10th International Conference on Microreaction Technology, IMRET 2008 - Topical Conference at the 2008 AIChE Spring National Meeting

Y2 - 1 April 2008 through 4 April 2008

ER -

Micro reactor application for the Beckmann rearrangement to epsilon-caprolactam

Abstract

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