Living cationic polymerizations utilizing an automated synthesizer : high-throughput synthesis of polyoxazolines

R. Hoogenboom, M.W.M. Fijten, M.A.R. Meier, U.S. Schubert

Research output: Contribution to journalArticleAcademicpeer-review

57 Citations (Scopus)

Abstract

Living cationic ring-opening polymerizations of 2-ethyl-2-oxazoline and purification of the resulting polymers were performed utilizing an automated synthesizer. Eight polymers (500 mg scale) as well as 40 polymers (150 mg scale) were synthesized in parallel to investigate the reproducibility and the living character of the polymerizations. The poly(2-ethyl-2-oxazoline)s obtained such were characterized by means of 1H NMR spectroscopy, MALDI-TOF mass spectrometry and online gel permeation chromatography.
Original languageEnglish
Pages (from-to)92-97
JournalMacromolecular Rapid Communications
Volume24
Issue number1
DOIs
Publication statusPublished - 2003

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