High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers

N. Adams; M. Moneke; S.A. Gulmus; D. Chenouf; M. Rehahn; U.S. Schubert

High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers

N. Adams, M. Moneke, S.A. Gulmus, D. Chenouf, M. Rehahn, U.S. Schubert

Department of Chemical Engineering and Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

8 Citations (Scopus)

Abstract

The development of novel polymer formulations is a complex as well as time and resource consuming task. To address this problem, a prodn.-size twin-screw extruder with four additive feeding units was coupled with a flat film extrusion line to yield an integrated system for combinatorial compounding (CC) and high throughput screening (HTS). This allows the rapid synthesis of polymer formulations of varying compns. When coupled to fast characterization equipment, this set-up will allow the discovery of polymer formulations in a high-throughput manner. A no. of possible rapid materials tests for screening purposes are discussed.

Original language	English
Title of host publication	Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.
Editors	M.J. Fasolka
Place of Publication	Warrendale, Pa
Publisher	Materials Research Society
Pages	171-179
ISBN (Print)	1-55899-848-9
Publication status	Published - 2006
Event	Combinatorial Methods and Informatics in Materials Science, November 28-December 1, 2005, Boston, MA, USA - Boston, MA, United States Duration: 28 Nov 2005 → 1 Dec 2005

Publication series

Name	Materials Research Society Symposium Proceedings
Volume	894
ISSN (Print)	0272-9172

Conference

Conference	Combinatorial Methods and Informatics in Materials Science, November 28-December 1, 2005, Boston, MA, USA
Country	United States
City	Boston, MA
Period	28/11/05 → 1/12/05
Other	Symposium held at the 2005 MRS Fall Meeting

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Adams, N., Moneke, M., Gulmus, S. A., Chenouf, D., Rehahn, M., & Schubert, U. S. (2006). High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. In M. J. Fasolka (Ed.), Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A. (pp. 171-179). (Materials Research Society Symposium Proceedings; Vol. 894). Materials Research Society.

Adams, N. ; Moneke, M. ; Gulmus, S.A. ; Chenouf, D. ; Rehahn, M. ; Schubert, U.S. / High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.. editor / M.J. Fasolka. Warrendale, Pa : Materials Research Society, 2006. pp. 171-179 (Materials Research Society Symposium Proceedings).

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title = "High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers",

abstract = "The development of novel polymer formulations is a complex as well as time and resource consuming task. To address this problem, a prodn.-size twin-screw extruder with four additive feeding units was coupled with a flat film extrusion line to yield an integrated system for combinatorial compounding (CC) and high throughput screening (HTS). This allows the rapid synthesis of polymer formulations of varying compns. When coupled to fast characterization equipment, this set-up will allow the discovery of polymer formulations in a high-throughput manner. A no. of possible rapid materials tests for screening purposes are discussed.",

author = "N. Adams and M. Moneke and S.A. Gulmus and D. Chenouf and M. Rehahn and U.S. Schubert",

year = "2006",

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series = "Materials Research Society Symposium Proceedings",

publisher = "Materials Research Society",

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booktitle = "Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.",

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note = "Combinatorial Methods and Informatics in Materials Science, November 28-December 1, 2005, Boston, MA, USA ; Conference date: 28-11-2005 Through 01-12-2005",

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Adams, N, Moneke, M, Gulmus, SA, Chenouf, D, Rehahn, M & Schubert, US 2006, High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. in MJ Fasolka (ed.), Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.. Materials Research Society Symposium Proceedings, vol. 894, Materials Research Society, Warrendale, Pa, pp. 171-179, Combinatorial Methods and Informatics in Materials Science, November 28-December 1, 2005, Boston, MA, USA, Boston, MA, United States, 28/11/05.

High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. / Adams, N.; Moneke, M.; Gulmus, S.A.; Chenouf, D.; Rehahn, M.; Schubert, U.S.

Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.. ed. / M.J. Fasolka. Warrendale, Pa : Materials Research Society, 2006. p. 171-179 (Materials Research Society Symposium Proceedings; Vol. 894).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

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T1 - High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers

AU - Adams, N.

AU - Moneke, M.

AU - Gulmus, S.A.

AU - Chenouf, D.

AU - Rehahn, M.

AU - Schubert, U.S.

PY - 2006

Y1 - 2006

N2 - The development of novel polymer formulations is a complex as well as time and resource consuming task. To address this problem, a prodn.-size twin-screw extruder with four additive feeding units was coupled with a flat film extrusion line to yield an integrated system for combinatorial compounding (CC) and high throughput screening (HTS). This allows the rapid synthesis of polymer formulations of varying compns. When coupled to fast characterization equipment, this set-up will allow the discovery of polymer formulations in a high-throughput manner. A no. of possible rapid materials tests for screening purposes are discussed.

AB - The development of novel polymer formulations is a complex as well as time and resource consuming task. To address this problem, a prodn.-size twin-screw extruder with four additive feeding units was coupled with a flat film extrusion line to yield an integrated system for combinatorial compounding (CC) and high throughput screening (HTS). This allows the rapid synthesis of polymer formulations of varying compns. When coupled to fast characterization equipment, this set-up will allow the discovery of polymer formulations in a high-throughput manner. A no. of possible rapid materials tests for screening purposes are discussed.

M3 - Conference contribution

SN - 1-55899-848-9

T3 - Materials Research Society Symposium Proceedings

SP - 171

EP - 179

BT - Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.

A2 - Fasolka, M.J.

PB - Materials Research Society

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T2 - Combinatorial Methods and Informatics in Materials Science, November 28-December 1, 2005, Boston, MA, USA

Y2 - 28 November 2005 through 1 December 2005

ER -

Adams N, Moneke M, Gulmus SA, Chenouf D, Rehahn M, Schubert US. High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. In Fasolka MJ, editor, Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.. Warrendale, Pa: Materials Research Society. 2006. p. 171-179. (Materials Research Society Symposium Proceedings).