High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers

N. Adams, M. Moneke, S.A. Gulmus, D. Chenouf, M. Rehahn, U.S. Schubert

Research output: Chapter in Book/Report/Conference proceedingConference contributionAcademicpeer-review

6 Citations (Scopus)

Abstract

The development of novel polymer formulations is a complex as well as time and resource consuming task. To address this problem, a prodn.-size twin-screw extruder with four additive feeding units was coupled with a flat film extrusion line to yield an integrated system for combinatorial compounding (CC) and high throughput screening (HTS). This allows the rapid synthesis of polymer formulations of varying compns. When coupled to fast characterization equipment, this set-up will allow the discovery of polymer formulations in a high-throughput manner. A no. of possible rapid materials tests for screening purposes are discussed.
Original languageEnglish
Title of host publicationCombinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.
EditorsM.J. Fasolka
Place of PublicationWarrendale, Pa
PublisherMaterials Research Society
Pages171-179
ISBN (Print)1-55899-848-9
Publication statusPublished - 2006
EventCombinatorial Methods and Informatics in Materials Science, November 28-December 1, 2005, Boston, MA, USA - Boston, MA, United States
Duration: 28 Nov 20051 Dec 2005

Publication series

NameMaterials Research Society Symposium Proceedings
Volume894
ISSN (Print)0272-9172

Conference

ConferenceCombinatorial Methods and Informatics in Materials Science, November 28-December 1, 2005, Boston, MA, USA
CountryUnited States
CityBoston, MA
Period28/11/051/12/05
OtherSymposium held at the 2005 MRS Fall Meeting

Fingerprint

Atom transfer radical polymerization
Copper
Polymers
Throughput
Catalysts
Screening
Extruders
Extrusion

Cite this

Adams, N., Moneke, M., Gulmus, S. A., Chenouf, D., Rehahn, M., & Schubert, U. S. (2006). High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. In M. J. Fasolka (Ed.), Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A. (pp. 171-179). (Materials Research Society Symposium Proceedings; Vol. 894). Warrendale, Pa: Materials Research Society.
Adams, N. ; Moneke, M. ; Gulmus, S.A. ; Chenouf, D. ; Rehahn, M. ; Schubert, U.S. / High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.. editor / M.J. Fasolka. Warrendale, Pa : Materials Research Society, 2006. pp. 171-179 (Materials Research Society Symposium Proceedings).
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abstract = "The development of novel polymer formulations is a complex as well as time and resource consuming task. To address this problem, a prodn.-size twin-screw extruder with four additive feeding units was coupled with a flat film extrusion line to yield an integrated system for combinatorial compounding (CC) and high throughput screening (HTS). This allows the rapid synthesis of polymer formulations of varying compns. When coupled to fast characterization equipment, this set-up will allow the discovery of polymer formulations in a high-throughput manner. A no. of possible rapid materials tests for screening purposes are discussed.",
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Adams, N, Moneke, M, Gulmus, SA, Chenouf, D, Rehahn, M & Schubert, US 2006, High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. in MJ Fasolka (ed.), Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.. Materials Research Society Symposium Proceedings, vol. 894, Materials Research Society, Warrendale, Pa, pp. 171-179, Combinatorial Methods and Informatics in Materials Science, November 28-December 1, 2005, Boston, MA, USA, Boston, MA, United States, 28/11/05.

High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. / Adams, N.; Moneke, M.; Gulmus, S.A.; Chenouf, D.; Rehahn, M.; Schubert, U.S.

Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.. ed. / M.J. Fasolka. Warrendale, Pa : Materials Research Society, 2006. p. 171-179 (Materials Research Society Symposium Proceedings; Vol. 894).

Research output: Chapter in Book/Report/Conference proceedingConference contributionAcademicpeer-review

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AB - The development of novel polymer formulations is a complex as well as time and resource consuming task. To address this problem, a prodn.-size twin-screw extruder with four additive feeding units was coupled with a flat film extrusion line to yield an integrated system for combinatorial compounding (CC) and high throughput screening (HTS). This allows the rapid synthesis of polymer formulations of varying compns. When coupled to fast characterization equipment, this set-up will allow the discovery of polymer formulations in a high-throughput manner. A no. of possible rapid materials tests for screening purposes are discussed.

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Adams N, Moneke M, Gulmus SA, Chenouf D, Rehahn M, Schubert US. High-throughput Experimentation Applied to Atom Transfer Radical Polymerization: Automated Optimization of the Copper Catalysts Removal from Polymers. In Fasolka MJ, editor, Combinatorial methods and informatics in materials science : symposium held November 28 - December 1, 2005, Boston, Massachusetts, U.S.A.. Warrendale, Pa: Materials Research Society. 2006. p. 171-179. (Materials Research Society Symposium Proceedings).