Flow synthesis of diaryliodonium triflates

G. Laudadio; H.P.L. Gemoets; T. Noël; V. Hessel

doi:10.1021/acs.joc.7b01346

Flow synthesis of diaryliodonium triflates

G. Laudadio, H.P.L. Gemoets, T. Noël, V. Hessel

Micro Flow Chemistry and Synthetic Meth.

Research output: Contribution to journal › Article › Academic › peer-review

32 Citations (Scopus)

119 Downloads (Pure)

Abstract

A safe and scalable synthesis of diaryliodonium triflates was achieved using a practical continuous-flow design. A wide array of electron-rich to electron-deficient arenes could readily be transformed to their respective diaryliodonium salts on a gram scale, with residence times varying from 2 to 60 s (44 examples).

Original language	English
Pages (from-to)	11735-11741
Number of pages	7
Journal	Journal of Organic Chemistry
Volume	82
Issue number	22
DOIs	https://doi.org/10.1021/acs.joc.7b01346
Publication status	Published - 17 Nov 2017

Keywords

Diaryliodonium Salts
Flow Chemistry

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10.1021/acs.joc.7b01346Licence: CC BY-NC-ND

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