Ethyl 5,5''-dimethyl-2,2';6',2''-terpyridine-4'-carboxylate

G. Kickelbick; R. Hoogenboom; U.S. Schubert

doi:10.1107/S1600536805038547

Ethyl 5,5''-dimethyl-2,2';6',2''-terpyridine-4'-carboxylate

G. Kickelbick, R. Hoogenboom, U.S. Schubert

Chemical Engineering and Chemistry

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Abstract

The title compound, C20H19N3O2, was synthesized by Stille coupling of ethyl 2,6-dibromoisonicotinate and 2-trimethylstannyl-5-methylpyridine. The three pyridine rings in the molecule are coplanar and the crystal packing reveals - stacking interactions between these conjugated aromatic rings with a distance between the mean planes of 3.494 Å.

Original language	English
Pages (from-to)	4322-4324
Number of pages	3
Journal	Acta Crystallographica, Section E: Structure Reports
Volume	61
Issue number	12
DOIs	https://doi.org/10.1107/S1600536805038547
Publication status	Published - 2005

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title = "Ethyl 5,5''-dimethyl-2,2';6',2''-terpyridine-4'-carboxylate",

abstract = "The title compound, C20H19N3O2, was synthesized by Stille coupling of ethyl 2,6-dibromoisonicotinate and 2-trimethylstannyl-5-methylpyridine. The three pyridine rings in the molecule are coplanar and the crystal packing reveals - stacking interactions between these conjugated aromatic rings with a distance between the mean planes of 3.494 {\AA}.",

author = "G. Kickelbick and R. Hoogenboom and U.S. Schubert",

year = "2005",

doi = "10.1107/S1600536805038547",

language = "English",

volume = "61",

pages = "4322--4324",

journal = "Acta Crystallographica, Section E: Structure Reports",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "12",

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T1 - Ethyl 5,5''-dimethyl-2,2';6',2''-terpyridine-4'-carboxylate

AU - Kickelbick, G.

AU - Hoogenboom, R.

AU - Schubert, U.S.

PY - 2005

Y1 - 2005

N2 - The title compound, C20H19N3O2, was synthesized by Stille coupling of ethyl 2,6-dibromoisonicotinate and 2-trimethylstannyl-5-methylpyridine. The three pyridine rings in the molecule are coplanar and the crystal packing reveals - stacking interactions between these conjugated aromatic rings with a distance between the mean planes of 3.494 Å.

AB - The title compound, C20H19N3O2, was synthesized by Stille coupling of ethyl 2,6-dibromoisonicotinate and 2-trimethylstannyl-5-methylpyridine. The three pyridine rings in the molecule are coplanar and the crystal packing reveals - stacking interactions between these conjugated aromatic rings with a distance between the mean planes of 3.494 Å.

U2 - 10.1107/S1600536805038547

DO - 10.1107/S1600536805038547

M3 - Article

VL - 61

SP - 4322

EP - 4324

JO - Acta Crystallographica, Section E: Structure Reports

JF - Acta Crystallographica, Section E: Structure Reports

SN - 1600-5368

IS - 12

ER -

Ethyl 5,5''-dimethyl-2,2';6',2''-terpyridine-4'-carboxylate

Abstract

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