Efficient routes to A3B-type meso -(4-carboxyphenyl) porphyrin derivatives

S.I. Presolski; R. Van Der Weegen; J. J. Wiesfeld; E. W. Meijer

doi:10.1021/ol500182z

Efficient routes to A₃B-type meso -(4-carboxyphenyl) porphyrin derivatives

S.I. Presolski
, R. Van Der Weegen
, J. J. Wiesfeld
, E. W. Meijer

Institute for Complex Molecular Systems

Research output: Contribution to journal › Article › Academic › peer-review

7 Citations (Scopus)

Abstract

A₃B-type meso-(4-carboxyphenyl) porphyrins were prepared either by stepwise coupling of aniline substituents to meso-tetrakis(4-carboxyphenyl) porphyrin (TCPP) or by utilizing its partially protected trimethyl ester derivative. We demonstrate the high utility of this building block, which can be synthesized in very good yields by microwave-assisted Me₃SnOH hydrolysis.

Original language	English
Pages (from-to)	1864-1867
Number of pages	4
Journal	Organic Letters
Volume	16
Issue number	7
DOIs	https://doi.org/10.1021/ol500182z
Publication status	Published - 4 Apr 2014

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10.1021/ol500182z

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abstract = "A3B-type meso-(4-carboxyphenyl) porphyrins were prepared either by stepwise coupling of aniline substituents to meso-tetrakis(4-carboxyphenyl) porphyrin (TCPP) or by utilizing its partially protected trimethyl ester derivative. We demonstrate the high utility of this building block, which can be synthesized in very good yields by microwave-assisted Me3SnOH hydrolysis.",

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AU - Presolski, S.I.

AU - Van Der Weegen, R.

AU - Wiesfeld, J. J.

AU - Meijer, E. W.

PY - 2014/4/4

Y1 - 2014/4/4

N2 - A3B-type meso-(4-carboxyphenyl) porphyrins were prepared either by stepwise coupling of aniline substituents to meso-tetrakis(4-carboxyphenyl) porphyrin (TCPP) or by utilizing its partially protected trimethyl ester derivative. We demonstrate the high utility of this building block, which can be synthesized in very good yields by microwave-assisted Me3SnOH hydrolysis.

AB - A3B-type meso-(4-carboxyphenyl) porphyrins were prepared either by stepwise coupling of aniline substituents to meso-tetrakis(4-carboxyphenyl) porphyrin (TCPP) or by utilizing its partially protected trimethyl ester derivative. We demonstrate the high utility of this building block, which can be synthesized in very good yields by microwave-assisted Me3SnOH hydrolysis.

UR - https://www.scopus.com/pages/publications/84898754145

U2 - 10.1021/ol500182z

DO - 10.1021/ol500182z

M3 - Article

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AN - SCOPUS:84898754145

SN - 1523-7060

VL - 16

SP - 1864

EP - 1867

JO - Organic Letters

JF - Organic Letters

IS - 7

ER -

Efficient routes to A₃B-type meso -(4-carboxyphenyl) porphyrin derivatives

Abstract

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