Development of a microrectification apparatus for analytical and preparative applications

A. Ziogas; V. Cominos; G.A. Kolb; H.J. Kost; B. Werner; V. Hessel

doi:10.1002/ceat.201100505

Development of a microrectification apparatus for analytical and preparative applications

A. Ziogas, V. Cominos, G.A. Kolb, H.J. Kost, B. Werner, V. Hessel

Micro Flow Chemistry and Synthetic Methodology

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Abstract

The realization of efficient microrectification equipment that can be operated intermittently or continuously is reported. The equipment can be used for both analytical and preparative separations of mixtures of liquid substances. Different binary systems were separated. A theoretical separation stage number of 12 was obtained, together with a height equivalent to one theoretical plate of 1.08¿cm. Compared to the state of microtechnology, this can be regarded as excellent progress.

Original language	English
Pages (from-to)	58-71
Number of pages	14
Journal	Chemical Engineering & Technology
Volume	35
Issue number	1
DOIs	https://doi.org/10.1002/ceat.201100505
Publication status	Published - 2012

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title = "Development of a microrectification apparatus for analytical and preparative applications",

abstract = "The realization of efficient microrectification equipment that can be operated intermittently or continuously is reported. The equipment can be used for both analytical and preparative separations of mixtures of liquid substances. Different binary systems were separated. A theoretical separation stage number of 12 was obtained, together with a height equivalent to one theoretical plate of 1.08¿cm. Compared to the state of microtechnology, this can be regarded as excellent progress.",

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AU - Ziogas, A.

AU - Cominos, V.

AU - Kolb, G.A.

AU - Kost, H.J.

AU - Werner, B.

AU - Hessel, V.

PY - 2012

Y1 - 2012

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AB - The realization of efficient microrectification equipment that can be operated intermittently or continuously is reported. The equipment can be used for both analytical and preparative separations of mixtures of liquid substances. Different binary systems were separated. A theoretical separation stage number of 12 was obtained, together with a height equivalent to one theoretical plate of 1.08¿cm. Compared to the state of microtechnology, this can be regarded as excellent progress.

U2 - 10.1002/ceat.201100505

DO - 10.1002/ceat.201100505

M3 - Article

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VL - 35

SP - 58

EP - 71

JO - Chemical Engineering & Technology

JF - Chemical Engineering & Technology

IS - 1

ER -

Development of a microrectification apparatus for analytical and preparative applications

Abstract

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