Design and test of a new high pressure phase equlibrium apparatus for highly corrosive mixtures of importance for natural gas

M. Mota Martinez; S. Samdani; A.S. Berrouk; M.A. Alves da Rocha; E.Y. Elhseinat; F. Banat; M.C. Kroon; C.J. Peters

doi:10.1016/j.jngse.2015.09.008

Design and test of a new high pressure phase equlibrium apparatus for highly corrosive mixtures of importance for natural gas

M. Mota Martinez, S. Samdani, A.S. Berrouk, M.A. Alves da Rocha, E.Y. Elhseinat, F. Banat, M.C. Kroon, C.J. Peters

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Abstract

A new static analytical apparatus for high-pressure phase equilibrium measurements has been designed and built. The new apparatus enables the measurement of vapor–liquid and liquid–liquid equilibria, which can operate at temperatures ranging from 225 K to 475 K and pressures up to 20 MPa. It is constructed in Titanium and alloy C276, being suitable for highly corrosive systems of interest for the gas industry (e.g., for hydrogen sulfide containing mixtures). The apparatus is equipped with two Rapid Online Sampling Injectors (ROLSI™) enabling the withdrawing of micro-samples without disturbing the equilibrium conditions. A gas chromatograph is connected to the apparatus for direct analysis of the phases' compositions. The quality and performance of the new apparatus has been evaluated by measuring a well reported system (carbon dioxide + methylcyclohexane).

Original language	English
Pages (from-to)	661-665
Number of pages	5
Journal	Journal of Natural Gas Science and Engineering
Volume	27
Issue number	2
DOIs	https://doi.org/10.1016/j.jngse.2015.09.008
Publication status	Published - 1 Nov 2015

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Mota Martinez, M., Samdani, S., Berrouk, A. S., Alves da Rocha, M. A., Elhseinat, E. Y., Banat, F., Kroon, M. C., & Peters, C. J. (2015). Design and test of a new high pressure phase equlibrium apparatus for highly corrosive mixtures of importance for natural gas. Journal of Natural Gas Science and Engineering, 27(2), 661-665. https://doi.org/10.1016/j.jngse.2015.09.008

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abstract = "A new static analytical apparatus for high-pressure phase equilibrium measurements has been designed and built. The new apparatus enables the measurement of vapor–liquid and liquid–liquid equilibria, which can operate at temperatures ranging from 225 K to 475 K and pressures up to 20 MPa. It is constructed in Titanium and alloy C276, being suitable for highly corrosive systems of interest for the gas industry (e.g., for hydrogen sulfide containing mixtures). The apparatus is equipped with two Rapid Online Sampling Injectors (ROLSI{\texttrademark}) enabling the withdrawing of micro-samples without disturbing the equilibrium conditions. A gas chromatograph is connected to the apparatus for direct analysis of the phases' compositions. The quality and performance of the new apparatus has been evaluated by measuring a well reported system (carbon dioxide + methylcyclohexane).",

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AU - Mota Martinez, M.

AU - Samdani, S.

AU - Berrouk, A.S.

AU - Alves da Rocha, M.A.

AU - Elhseinat, E.Y.

AU - Banat, F.

AU - Kroon, M.C.

AU - Peters, C.J.

PY - 2015/11/1

Y1 - 2015/11/1

N2 - A new static analytical apparatus for high-pressure phase equilibrium measurements has been designed and built. The new apparatus enables the measurement of vapor–liquid and liquid–liquid equilibria, which can operate at temperatures ranging from 225 K to 475 K and pressures up to 20 MPa. It is constructed in Titanium and alloy C276, being suitable for highly corrosive systems of interest for the gas industry (e.g., for hydrogen sulfide containing mixtures). The apparatus is equipped with two Rapid Online Sampling Injectors (ROLSI™) enabling the withdrawing of micro-samples without disturbing the equilibrium conditions. A gas chromatograph is connected to the apparatus for direct analysis of the phases' compositions. The quality and performance of the new apparatus has been evaluated by measuring a well reported system (carbon dioxide + methylcyclohexane).

AB - A new static analytical apparatus for high-pressure phase equilibrium measurements has been designed and built. The new apparatus enables the measurement of vapor–liquid and liquid–liquid equilibria, which can operate at temperatures ranging from 225 K to 475 K and pressures up to 20 MPa. It is constructed in Titanium and alloy C276, being suitable for highly corrosive systems of interest for the gas industry (e.g., for hydrogen sulfide containing mixtures). The apparatus is equipped with two Rapid Online Sampling Injectors (ROLSI™) enabling the withdrawing of micro-samples without disturbing the equilibrium conditions. A gas chromatograph is connected to the apparatus for direct analysis of the phases' compositions. The quality and performance of the new apparatus has been evaluated by measuring a well reported system (carbon dioxide + methylcyclohexane).

U2 - 10.1016/j.jngse.2015.09.008

DO - 10.1016/j.jngse.2015.09.008

M3 - Article

SN - 1875-5100

VL - 27

SP - 661

EP - 665

JO - Journal of Natural Gas Science and Engineering

JF - Journal of Natural Gas Science and Engineering

IS - 2

ER -

Design and test of a new high pressure phase equlibrium apparatus for highly corrosive mixtures of importance for natural gas

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