Characterization of chemically bonded phases on precoated thin-layer plates by 29Si and 13C cross-polarization and magic-angle spinning NMR

J.W. Haan, de; L.J.M. Ven, van de; G. Vries, de; U.A.T. Brinkman

doi:10.1007/BF02313680

Characterization of chemically bonded phases on precoated thin-layer plates by 29Si and 13C cross-polarization and magic-angle spinning NMR

J.W. Haan, de
, L.J.M. Ven, van de
, G. Vries, de
, U.A.T. Brinkman

Research output: Contribution to journal › Article › Academic › peer-review

5 Citations (Scopus)

216 Downloads (Pure)

Abstract

The paper reports results for commercial precoated plates and home-made bonded phases for TLC examined by29Si and13C NMR of solid samples. The NMR spectra readily reveal differences in degree of silylation, details pertaining to the type of reactive silanes used, and differences in the methods of synthesis. They can also be used to explain the cause of the wettability problems encountered with some types of (precoated) TLC plates.

Original language	English
Pages (from-to)	687-692
Journal	Chromatographia
Volume	21
Issue number	12
DOIs	https://doi.org/10.1007/BF02313680
Publication status	Published - 1986

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title = "Characterization of chemically bonded phases on precoated thin-layer plates by 29Si and 13C cross-polarization and magic-angle spinning NMR",

abstract = "The paper reports results for commercial precoated plates and home-made bonded phases for TLC examined by29Si and13C NMR of solid samples. The NMR spectra readily reveal differences in degree of silylation, details pertaining to the type of reactive silanes used, and differences in the methods of synthesis. They can also be used to explain the cause of the wettability problems encountered with some types of (precoated) TLC plates.",

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year = "1986",

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pages = "687--692",

journal = "Chromatographia",

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T1 - Characterization of chemically bonded phases on precoated thin-layer plates by 29Si and 13C cross-polarization and magic-angle spinning NMR

AU - Haan, de, J.W.

AU - Ven, van de, L.J.M.

AU - Vries, de, G.

AU - Brinkman, U.A.T.

PY - 1986

Y1 - 1986

N2 - The paper reports results for commercial precoated plates and home-made bonded phases for TLC examined by29Si and13C NMR of solid samples. The NMR spectra readily reveal differences in degree of silylation, details pertaining to the type of reactive silanes used, and differences in the methods of synthesis. They can also be used to explain the cause of the wettability problems encountered with some types of (precoated) TLC plates.

AB - The paper reports results for commercial precoated plates and home-made bonded phases for TLC examined by29Si and13C NMR of solid samples. The NMR spectra readily reveal differences in degree of silylation, details pertaining to the type of reactive silanes used, and differences in the methods of synthesis. They can also be used to explain the cause of the wettability problems encountered with some types of (precoated) TLC plates.

U2 - 10.1007/BF02313680

DO - 10.1007/BF02313680

M3 - Article

SN - 0009-5893

VL - 21

SP - 687

EP - 692

JO - Chromatographia

JF - Chromatographia

IS - 12

ER -

Characterization of chemically bonded phases on precoated thin-layer plates by 29Si and 13C cross-polarization and magic-angle spinning NMR

Abstract

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