Brittle fracture-based experimental methodology for microstructure analysis

J.P.M. Hoefnagels, C.C. Tasan, M. Pradelle, M.G.D. Geers

Research output: Chapter in Book/Report/Conference proceedingChapterAcademicpeer-review

4 Citations (Scopus)
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Abstract

Metallographic techniques are crucial tools for establishing the connection between observed mechanical behaviour of metals and the underlying mechanisms in their microstructures. In this work, we propose a methodology that minimizes deformation and/or modification of the microstructure during specimen preparation, and provides a 3D representation of the deformed micromorphology. This methodology involves opening up fractured (tensile test) specimens under the ductile-to-brittle transition temperature of metals to yield two parts in a brittle manner. The occurrence of brittle fracture is validated by analyzing the detailed, unaltered microstructure from SEM characterization and surface profilometry mapping of sets of two parts. It is found that this technique yields additional valuable information regarding the size and morphology of deformed grains or nucleation mechanisms of ductile damage. Experiments with a number of different steels show that the methodology can be applied to sheet of different formability.
Original languageEnglish
Title of host publicationAdvanced in Experimental Mechanics VI
EditorsJ.M. Dulieu-Barton, D. Lord, R.J. Greene
Place of PublicationZurich
PublisherTrans Tech Publications
Pages133-139
ISBN (Print)978-0-87849-367-8
DOIs
Publication statusPublished - 2008

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brittle fracture
microstructure
methodology
micromorphology
metal
nucleation
steel
scanning electron microscopy
damage
analysis
experiment
temperature

Cite this

Hoefnagels, J. P. M., Tasan, C. C., Pradelle, M., & Geers, M. G. D. (2008). Brittle fracture-based experimental methodology for microstructure analysis. In J. M. Dulieu-Barton, D. Lord, & R. J. Greene (Eds.), Advanced in Experimental Mechanics VI (pp. 133-139). Zurich: Trans Tech Publications. https://doi.org/10.4028/www.scientific.net/AMM.13-14.133
Hoefnagels, J.P.M. ; Tasan, C.C. ; Pradelle, M. ; Geers, M.G.D. / Brittle fracture-based experimental methodology for microstructure analysis. Advanced in Experimental Mechanics VI. editor / J.M. Dulieu-Barton ; D. Lord ; R.J. Greene. Zurich : Trans Tech Publications, 2008. pp. 133-139
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Hoefnagels, JPM, Tasan, CC, Pradelle, M & Geers, MGD 2008, Brittle fracture-based experimental methodology for microstructure analysis. in JM Dulieu-Barton, D Lord & RJ Greene (eds), Advanced in Experimental Mechanics VI. Trans Tech Publications, Zurich, pp. 133-139. https://doi.org/10.4028/www.scientific.net/AMM.13-14.133

Brittle fracture-based experimental methodology for microstructure analysis. / Hoefnagels, J.P.M.; Tasan, C.C.; Pradelle, M.; Geers, M.G.D.

Advanced in Experimental Mechanics VI. ed. / J.M. Dulieu-Barton; D. Lord; R.J. Greene. Zurich : Trans Tech Publications, 2008. p. 133-139.

Research output: Chapter in Book/Report/Conference proceedingChapterAcademicpeer-review

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Hoefnagels JPM, Tasan CC, Pradelle M, Geers MGD. Brittle fracture-based experimental methodology for microstructure analysis. In Dulieu-Barton JM, Lord D, Greene RJ, editors, Advanced in Experimental Mechanics VI. Zurich: Trans Tech Publications. 2008. p. 133-139 https://doi.org/10.4028/www.scientific.net/AMM.13-14.133