Brittle-ductile transition temperature of recrystallized tungsten following exposure to fusion relevant cyclic high heat load

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Abstract

The lifetime of tungsten (W) monoblocks under fusion conditions is ambivalent. In this work, the microstructure dependent mechanical behaviour of pulsed high heat flux (HHF) exposed W monoblock is investigated. Two different microstructural states, i.e. initial (deformed) and recrystallized, both machined from HHF exposed monoblocks are tested using tensile and small punch tests. The initial microstructural state reveals a higher fraction of low angle boundaries along with a preferred orientation of crystals. Following HHF exposure, the recrystallized state exhibits weakening of initial texture along with a higher fraction of high angle boundaries. Irrespective of the testing methodology, both the microstructural states display brittle failure for temperatures lower than 400∘C. For higher temperatures (>400∘C), the recrystallized microstructure exhibits more ductile behaviour as compared to the initial state. The observed microstructural state-dependent mechanical behaviour is further discussed in terms of different microstructural features. The estimated brittle-to-ductile transition temperature (BDTT) range is noticed to be lower for the recrystallized state as compared to the initial state. The lower BDTT in the recrystallized state is attributed to the high purity of the W in combination with its low defect density, thereby preventing segregation of impurities at the recrystallized boundaries and the related premature failure. Based on this observation, it is concluded that the common opinion of the aggravation of BDTT in W due to recrystallization is not unerring, and as a matter of fact, recrystallization in W could be instrumental for preventing the self-castellation of the monoblocks.
Original languageEnglish
Article number152416
Number of pages16
JournalJournal of Nuclear Materials
Volume541
DOIs
Publication statusPublished - 1 Dec 2020

Funding

This research was carried out under project number T16010c in the framework of the Research Program of the Materials innovation institute (M2i) (www.m2i.nl) supported by the Dutch government and, within the framework of the EUROfusion Consortium and has received funding from the Euratom research and training programme 2014-2018 and 2019-2020 under grant agreement No 633053. The views and opinions expressed herein do not necessarily reflect those of the European Commission. The authors would like to thank RI Research Instruments GmbH in Germany for supplying the high heat flux exposed monoblock samples. The help of Mario Houska and Wolfgang Webersinke (Helmholtz-Zentrum Dresden-Rossendorf, Germany) in performing the high temperature tensile and small punch test is greatly acknowledged. Additionally, the assistance of Marc van Maris from the Multi-Scale lab (Eindhoven University of Technology, The Netherlands) is highly appreciated. This research was carried out under project number T16010c in the framework of the Research Program of the Materials innovation institute (M2i) (www.m2i.nl) supported by the Dutch government and, within the framework of the EUROfusion Consortium and has received funding from the Euratom research and training programme 2014-2018 and 2019-2020 under grant agreement No 633053. The views and opinions expressed herein do not necessarily reflect those of the European Commission. The authors would like to thank RI Research Instruments GmbH in Germany for supplying the high heat flux exposed monoblock samples. The help of Mario Houska and Wolfgang Webersinke (Helmholtz-Zentrum Dresden-Rossendorf, Germany) in performing the high temperature tensile and small punch test is greatly acknowledged. Additionally, the assistance of Marc van Maris from the Multi-Scale lab (Eindhoven University of Technology, The Netherlands) is highly appreciated.

FundersFunder number
Helmholtz-Zentrum Dresden-Rossendorf
European Union's Horizon 2020 - Research and Innovation Framework Programme633053
Eindhoven University of Technology
Materials Innovation Institute (M2i)

    Keywords

    • Brittle-to-ductile transition temperature (BDTT)
    • High Heat Flux (HHF) exposure
    • Recrystallization and embrittlement
    • Tensile and small punch test
    • Tungsten

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