Application of a parallel synthetic approach in atom-transfer radical polymerization : set-up and feasibility demonstration

H. Zhang; M.W.M. Fijten; R. Hoogenboom; R.B.J.M. Reinierkens; U.S. Schubert

doi:10.1002/marc.200390002

Application of a parallel synthetic approach in atom-transfer radical polymerization : set-up and feasibility demonstration

H. Zhang
, M.W.M. Fijten
, R. Hoogenboom
, R.B.J.M. Reinierkens
, U.S. Schubert

Chemical Engineering and Chemistry

Research output: Contribution to journal › Article › Academic › peer-review

55 Citations (Scopus)

Abstract

A parallel synthetic approach toward homogeneous atom-transfer radical polymerization of methyl methacrylate has been successfully applied by utilizing an automated synthesizer. Experimental set-up, automated parallel synthesis and purification of the polymers via a solid-phase extraction set-up, as well as online and offline measurements of the molecular weights and monomer conversion are described in detail. In addition, a comparison with conventional experiments in the laboratory is provided.

Original language	English
Pages (from-to)	81-86
Journal	Macromolecular Rapid Communications
Volume	24
Issue number	1
DOIs	https://doi.org/10.1002/marc.200390002
Publication status	Published - 2003

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10.1002/marc.200390002

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abstract = "A parallel synthetic approach toward homogeneous atom-transfer radical polymerization of methyl methacrylate has been successfully applied by utilizing an automated synthesizer. Experimental set-up, automated parallel synthesis and purification of the polymers via a solid-phase extraction set-up, as well as online and offline measurements of the molecular weights and monomer conversion are described in detail. In addition, a comparison with conventional experiments in the laboratory is provided.",

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AU - Reinierkens, R.B.J.M.

AU - Schubert, U.S.

PY - 2003

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AB - A parallel synthetic approach toward homogeneous atom-transfer radical polymerization of methyl methacrylate has been successfully applied by utilizing an automated synthesizer. Experimental set-up, automated parallel synthesis and purification of the polymers via a solid-phase extraction set-up, as well as online and offline measurements of the molecular weights and monomer conversion are described in detail. In addition, a comparison with conventional experiments in the laboratory is provided.

U2 - 10.1002/marc.200390002

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JO - Macromolecular Rapid Communications

JF - Macromolecular Rapid Communications

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Application of a parallel synthetic approach in atom-transfer radical polymerization : set-up and feasibility demonstration

Abstract

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