A mild, one-pot Stadler–Ziegler synthesis of arylsulfides facilitated by photoredox catalysis in batch and continuous-flow

X. Wang, Gregory D. Cuny, T. Noel

Research output: Contribution to journalArticleAcademicpeer-review

136 Citations (Scopus)
1 Downloads (Pure)

Abstract

Visible advance: A mild, one-pot Stadler–Ziegler process for CS bond formation has been developed. The method employs the photoredox catalyst [Ru(bpy)3Cl2]·6¿H2O irradiated with visible light. A variety of aryl–alkyl and diaryl sulfides were prepared from readily available arylamines and aryl/alkylthiols in good yields. The use of a photo microreactor led to a significant improvement with respect to safety and efficiency
Original languageEnglish
Pages (from-to)7860-7864
Number of pages5
JournalAngewandte Chemie - International Edition
Volume52
Issue number30
DOIs
Publication statusPublished - 2013

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