A mild, one-pot Stadler–Ziegler synthesis of arylsulfides facilitated by photoredox catalysis in batch and continuous-flow

X. Wang; Gregory D. Cuny; T. Noel

doi:10.1002/anie.201303483

A mild, one-pot Stadler–Ziegler synthesis of arylsulfides facilitated by photoredox catalysis in batch and continuous-flow

X. Wang, Gregory D. Cuny, T. Noel

Micro Flow Chemistry and Synthetic Methodology

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Abstract

Visible advance: A mild, one-pot Stadler–Ziegler process for CS bond formation has been developed. The method employs the photoredox catalyst [Ru(bpy)3Cl2]·6¿H2O irradiated with visible light. A variety of aryl–alkyl and diaryl sulfides were prepared from readily available arylamines and aryl/alkylthiols in good yields. The use of a photo microreactor led to a significant improvement with respect to safety and efficiency

Original language	English
Pages (from-to)	7860-7864
Number of pages	5
Journal	Angewandte Chemie - International Edition
Volume	52
Issue number	30
DOIs	https://doi.org/10.1002/anie.201303483
Publication status	Published - 2013

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title = "A mild, one-pot Stadler–Ziegler synthesis of arylsulfides facilitated by photoredox catalysis in batch and continuous-flow",

abstract = "Visible advance: A mild, one-pot Stadler–Ziegler process for CS bond formation has been developed. The method employs the photoredox catalyst [Ru(bpy)3Cl2]·6¿H2O irradiated with visible light. A variety of aryl–alkyl and diaryl sulfides were prepared from readily available arylamines and aryl/alkylthiols in good yields. The use of a photo microreactor led to a significant improvement with respect to safety and efficiency",

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AU - Wang, X.

AU - Cuny, Gregory D.

AU - Noel, T.

PY - 2013

Y1 - 2013

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AB - Visible advance: A mild, one-pot Stadler–Ziegler process for CS bond formation has been developed. The method employs the photoredox catalyst [Ru(bpy)3Cl2]·6¿H2O irradiated with visible light. A variety of aryl–alkyl and diaryl sulfides were prepared from readily available arylamines and aryl/alkylthiols in good yields. The use of a photo microreactor led to a significant improvement with respect to safety and efficiency

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DO - 10.1002/anie.201303483

M3 - Article

C2 - 23784666

SN - 0570-0833

VL - 52

SP - 7860

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JO - Angewandte Chemie - International Edition

JF - Angewandte Chemie - International Edition

IS - 30

ER -

A mild, one-pot Stadler–Ziegler synthesis of arylsulfides facilitated by photoredox catalysis in batch and continuous-flow

Abstract

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