A heatable stretching device for dynamic X-ray studies

N.A.J.M. Aerle, van; A.W.M. Braam

doi:10.1107/S0021889887010057

A heatable stretching device for dynamic X-ray studies

N.A.J.M. Aerle, van, A.W.M. Braam

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Abstract

In this paper a heatable stretching device is presented which enables the performance of real-time X-ray experiments during deformation. The construction of the oven makes it possible to perform experiments with detectable X-ray diffraction angles (2) of up to 30°. It is shown that the apparatus can be used to study morphological changes occurring during the deformation/drawing of polymer materials, using the benefits of synchrotron facilities. A series of small-angle (SAXS) and wide-angle (WAXS) X-ray scattering patterns obtained during the drawing of melt-crystallized ultra-high-molecular-weight polyethylene (UHMW-PE) at 373 K is presented.

Original language	English
Pages (from-to)	106-108
Number of pages	3
Journal	Journal of Applied Crystallography
Volume	21
Issue number	2
DOIs	https://doi.org/10.1107/S0021889887010057
Publication status	Published - 1988

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title = "A heatable stretching device for dynamic X-ray studies",

abstract = "In this paper a heatable stretching device is presented which enables the performance of real-time X-ray experiments during deformation. The construction of the oven makes it possible to perform experiments with detectable X-ray diffraction angles (2) of up to 30°. It is shown that the apparatus can be used to study morphological changes occurring during the deformation/drawing of polymer materials, using the benefits of synchrotron facilities. A series of small-angle (SAXS) and wide-angle (WAXS) X-ray scattering patterns obtained during the drawing of melt-crystallized ultra-high-molecular-weight polyethylene (UHMW-PE) at 373 K is presented.",

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AU - Aerle, van, N.A.J.M.

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AB - In this paper a heatable stretching device is presented which enables the performance of real-time X-ray experiments during deformation. The construction of the oven makes it possible to perform experiments with detectable X-ray diffraction angles (2) of up to 30°. It is shown that the apparatus can be used to study morphological changes occurring during the deformation/drawing of polymer materials, using the benefits of synchrotron facilities. A series of small-angle (SAXS) and wide-angle (WAXS) X-ray scattering patterns obtained during the drawing of melt-crystallized ultra-high-molecular-weight polyethylene (UHMW-PE) at 373 K is presented.

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DO - 10.1107/S0021889887010057

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EP - 108

JO - Journal of Applied Crystallography

JF - Journal of Applied Crystallography

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ER -

A heatable stretching device for dynamic X-ray studies

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